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Table 3.
Registration parameters of NMR 1H and 2H spectra.
Parameter | 1H | 2H |
---|---|---|
The angle of the | 90∘ | 90∘ |
excitation pulse | ||
Acquisition time | 3.5 sec | 1.9 sec |
Relaxation delay | 17 sec | 0.5 sec* |
Spectrum width | 15 ppm | 25 ppm |
Points number | 32 K | 4 K |
Scans number | 8 | 256 |
Exponential multiplication | 0.2 Hz | 2.0 Hz |
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